有機化學裝置的制造及其處理,應用技術
  • 本發明涉及的是新化合物及這些化合物與金屬的新配合物。本發明的新化合物及配合物可用于疾病的診斷和治療方法。金屬配合物,如含放射性金屬的那些配合物作為診斷試劑和治療劑正在有發現越來越多的用途。其中特別令人感興趣的是那些含有能夠被所需部位選擇性吸收以便于評定和治療受試體的生物活性部分的配合物。本...
  • 本發明涉及生產包括紫杉醇的紫杉烷型雙萜的方法,紫杉醇是用于治療卵巢癌、乳癌、肺癌等的很好的藥劑。用于卵巢癌、乳癌、肺癌等的治療藥劑的紫杉醇是一種從短葉紫杉NUTT中分離出來后被鑒別出的紫杉烷(taxane)型雙萜,紫杉是一種屬于紫杉屬紫杉科族的植物,紫杉醇有一個與上述藥理活性有關的復雜的酯基。可以...
  • 本發明涉及在催化劑存在下、水溶液中水合不飽合醛制造羥基烷醛的方法。以往,作為將不飽和醛之一的丙烯醛在催化劑存在下,水溶液中進行水合,制取羥基烷醛之一的3-羥基丙醛方法有以下的各種制造方法。即,在USP2,434,110號中公開了使用硫酸等的無機酸作為上述反應系統中酸性均相催化劑的方法。但是這種方法...
  • 本發明涉及在液態氨中由二苯酮制備二苯酮亞胺的方法。在熔融形式的或在溶液中的二苯酮與氣態或液態氨的直接反應中,作為催化劑必須加入氯化鐵(III)(JP-A-61/030563,產率57%)、有機酸,如苯甲酸(US-A-4130586,產率18-65%)或氯化銨(SyntheticCommunica...
  • 本發明涉及如下通式的哌嗪衍生物,互變異構體,立體異構體,包括其混合物及其鹽,特別是具有藥物可接受的酸或堿的鹽,它們具有有效的藥理性能,尤其是抑制聚集作用的效果,本發明還涉及含這些化合物的藥物組合物及其用途以及其制備方法。在上述通式I中的先決條件是假若Ra表示4-吡啶基時,則不可能同時(a)Y1表...
  • 本發明涉及具有骨生成促進活性、骨吸收抑制活性和其他活性的光學活性苯并硫雜庚英衍生物,和含有其作為活性成分的骨疾病預防或治療藥物。骨疾病是一種涉及由骨量減少超過某一程度引起的某些癥狀或傾向的病理狀態或疾病。骨質疏松(一種骨疾病)的主要癥狀是脊柱后凸,和背腰骨、椎骨體、股骨頸、橈骨下端、肋骨、肱骨上端...
  • 本發明涉及從含(甲基)丙烯酸和沸點高于(甲基)丙烯酸的惰性疏水有機液體為主要成分和還含有低級醛為次要成分的混合物中精餾分離(甲基)丙烯酸的新方法。(甲基)丙烯酸是簡寫,表示丙烯酸或甲基丙烯酸。(甲基)丙烯酸本身或它的各種形式的酯對制備具有非常廣泛用途,例如粘合劑的聚合物是特別重要的。(甲基)丙烯酸...
  • 本發明涉及制備丙烯酸的方法,尤其,本發明涉及一種在特定條件下制得的鉬/釩基氧化物催化劑存在下,使用分子氧或含分子氧的氣體,通過氣相催化氧化丙烯醛或含丙烯醛的氣體來制備丙烯酸的方法。多種改進的催化劑被推薦用于通過氣相催化氧化丙烯醛來有效地制備丙烯酸。其中大多數量是含鉬和釩作為主要成分的鉬/釩基催化劑...
  • 本發明涉及用于異丁烯醛氣相氧化制備異丁烯酸的新催化劑,異丁烯醛是通過異丁烯或叔丁醇氣相催化氧化得到的。據報道,有多種催化劑可作為異丁烯醛氣相氧化制備異丁烯酸的催化劑,尤其是在許多專利公開出版物中報道了雜多酸衍生物作為制備異丁烯酸的催化劑。然而,由于包括雜多酸衍生物的催化劑自身的性質,使它們具有一些...
  • 本發明是屬于合成氣一步制取二甲醚的方法,特別是所用的催化劑及其制備過程。二甲醚不僅是從合成氣經由甲醇轉化制汽油改良法的主要中間體,而且是生產多種化工產品的重要原料,并在制藥、染料、農藥等工業中有許多獨特的用途。二甲醚還可能作為一種城市煤氣或液化氣甚至柴油的代用品而日益引起重視。由合成氣一步制取二甲...
  • 本發明涉及借助1,1-二氟四鹵代乙烷與醇的反應直接制備鹵代二氟乙酸烷基酯的方法。鹵代二氟乙酸烷基酯是合成藥物和植物保健產品的中間體。獲得這些鹵代二氟乙酸烷基酯的方法已經記載了很多。這些方法中最普遍采用的是醇與鹵代二氟乙酸反應,或優選與相應的氟化物和氯化物反應。根據大量的各種技術方法可以得到這些鹵代...
  • 本發明涉及鏈烷磺酸的合成,具體地本發明的內容在于,由相應的含硫衍生物制備C1-C4鏈烷磺酸。鏈烷磺酸及其鹽在工業上有許多應用,具體如洗滌劑,乳化劑,酯化催化劑,以及某些樹脂的硬化劑。工業上,鏈烷磺酸往往是由鏈烷經磺化作用或氯磺化作用制備的。然而這兩種合成方法的缺點是導致在烴鏈的不同碳原子上生成磺化...
  • 本發明涉及新的1-環丙基四唑啉酮,它們的制備方法,它們作為除草劑的用途,及其制備過程中新的中間體和它們的制備方法。已知某些取代的四唑啉酮具有除草活性[見美國專利4,618,365(=EP-A-146,279);4,826,529;4,830,661;4,956,469;5,003,075;5,01...
  • 本發明涉及一種,該方法包括由1,3-二氯苯經二硝基化得到1,3′-二氯-4,6/2,4-二硝基苯混合物,接著與芐醇鈉(Sodiumbenzylate)反應得到1,3-二芐氧基-4,6-二硝基苯和催化氫化。4,6-二氨基間苯二酚是塑料的重要單體結構單元,特別是組成聚苯并噁唑的重要單體(高分子,19...
  • 本發明涉及1-氧代-2-(苯磺酰氨基)戊基哌啶衍生物,其制備方法及其藥用。本發明化合物如下式(I)所示其中R1是氫或(C1-C4)烷基,R2是氫或直鏈或支鏈(C1-C4)烷基,R3是直鏈或支鏈(C1-C7)烷基,-(CH2)nOCH3基團(其中n是1,2或3)或-CH2O(C2H4O)mCH3(...
  • 本發明涉及D-氨基酸的立體控制合成方法。下式(1)代表D-氨基酸-N-(S)-α-烷基芐基酰胺中,R1是甲基、乙基或異丙基及R2是甲基或乙基的化合物是重要的物質,它們可用作具有強甜度的物質的中間體,見US.5286509中所述。所述式(1)如下式中標有*的碳原子具有D-氨基酸結構,R1是具有1至...
  • 本發明涉及由有機伯胺與碳酰氯在有機溶劑中、于60-100℃溫度下反應,其中反應混合物通過泡罩塔進行循環。通過使有機伯胺與碳酰氯在有機溶劑中反應連續制備有機異氰酸酯的方法已在多處介紹過,并已大規模進行生產(例如,參見UllmannsEnzyklopdiederTechnischenChem...
  • 本發明涉及通式I的11β-芳基-4-雌烯及其藥物上適宜的酸加成鹽,以及它們的制備方法、含有該化合物的藥物組合物、在制備藥物上的應用和為此所需的新的中間產物,式中X表示氧原子,肟基N-OH或2個氫原子,R1表示氫原子或甲基,R2表示羥基,C1-C10-烷氧基-或C1-C10酰氧基,R3表示氫原子、...
  • 本發明涉及通過特定的縮合反應由醛制備β-酮醇的新方法以及此方法制得的一些新產物。ChemistryLetters1991,1377-1378(Inoue等人)披露了環狀α-甲叉基碳酸酯即4,4-二甲基-5-甲叉基-1,3-二氧戊環-2-酮(以下稱“環碳酸酯”)和芳醛之間環化加成反應,裂解掉二氧...
  • 本發明涉及可用于將氨基酸轉化成鹵代甲基酮然后又轉化成氨基酸環氧化物的新方法。這樣的環氧化物是合成腎素和HIV蛋白酶的抑制劑的重要的中間體。所述腎素和HIV蛋白酶的抑制劑尤其可用于治療和/或預防HIV感染(AIDS)。氨基酸α-鹵代甲基酮除可用作某些含半胱氨酸和絲氨酸的蛋白酶的不可逆的活性部位的抑制...
技術分類
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